INDUSTRY 16

Glycol Concentration Meter

16 / DATA CENTER

Inline EG / PG concentration for AI liquid-cooled data centers — cold-plate and immersion, plus metro and commercial HVAC chiller applications.

2 applicable products 1 application cases

Overview

AI workloads have driven per-rack power from 5-15 kW to 50-150 kW, making liquid cooling (cold plate, immersion, in-row) the default for new hyperscale data centers. Loops run ethylene glycol (EG, 30-50 vol%) or propylene glycol (PG) in water. Too lean: dry coolers freeze and burst in winter (single incident worth millions plus SLA penalties). Too rich: viscosity rises, heat-transfer efficiency falls, pump energy +5-10%. PS7400 inline tuning-fork density monitors EG / PG concentration continuously — a core instrument for Alibaba, Tencent, ByteDance, Huawei and the three-carrier IDC operators. Same approach covers HVAC scenarios: metro ventilation chillers, commercial cooling, chemical cooling and ice-storage systems.

Process challenges

  • EG concentration drifts continuously — water evaporation + glycol oxidation + operator top-up bias, accumulating 5-10% over 3-5 years
  • IDC operators are network specialists, not chemists — monthly handheld-refractometer sampling can't catch drift
  • Tier 3/4 facilities need long-life unmaintained sensors — instrument failure means downtime
  • HVAC pipe sizes vary widely (DN50-DN200), needing flexible installation
  • Glycol operates 5-45°C — automatic temperature compensation is mandatory
  • A PG loop grows biofilm more readily than an EG loop — propylene glycol is far more biodegradable than ethylene glycol, which is exactly why it is preferred on toxicity grounds, but in a warm closed loop that makes it a nutrient
  • Refractive index cannot tell PG from EG: at 25 vol% the two differ by about 0.0002 RI, while 1 vol% of concentration is about 0.001 RI. The instrument has to be told which fluid it is reading, and the make-up fluid has to be confirmed explicitly at commissioning and written into the checklist

Why a PG loop has to go optical

EG and PG are not the same selection problem. Refractive index is monotonic across the range for both; sound velocity is monotonic for EG over the working range but folds back for PG — it turns over, and one sound velocity then corresponds to two concentrations. There is no acoustic route to PG.

CoolantTuning fork PS7400Sound velocity PS7020Refractometer PS7110
EG (ethylene glycol)YesYesYes
PG (propylene glycol)YesNo — sound velocity turns overYes

Glycols move refractive index by roughly 0.001 RI per vol%. The PS7110 is specified at ±0.0001 RI, which works out at ±0.1 vol%; its 0.00001 RI resolution works out at 0.01 vol%. Typical operating points — PG10 ≈ 1.343, PG25 ≈ 1.358, PG40 ≈ 1.373, EG30 ≈ 1.363 — all sit in the lower third of the PS7110-B range (1.33299–1.51782), with headroom on both sides. The prism face is rated to 1.5 MPa against a typical CDU secondary loop at 6 bar or less.

Temperature is what picks the variant. The PS7110-B runs 0–70 °C, which covers an indoor CDU secondary loop at 10–60 °C — but its lower limit is 0 °C, not below zero. An outdoor dry-cooler loop can fall below 0 °C in winter, and that duty needs the PS7110-C (−10 to 100 °C). Saying so plainly is how the wrong variant stops being ordered.

One limitation belongs in the open: refractive index cannot tell PG from EG. At 25 vol% the two differ by about 0.0002 RI, while 1 vol% of concentration is about 0.001 RI — the gap between the two liquids is a fifth of the smallest concentration step that means anything. The consequence is concrete: top a PG loop up with EG and the instrument returns a perfectly plausible wrong number, and raises no fault doing it. That is not a sensor defect, it is a configuration and procedure problem, and it has a concrete answer. The fluid must be declared to the instrument rather than guessed at; it should be selectable over Modbus and readable back for verification; and it should be confirmed explicitly at commissioning and written into the checklist.

A change of inhibitor package is not a worry: dissolved solids move refractive index by about 0.0001–0.0002 RI/wt%, which against a 0.001 RI/vol% concentration slope is an offset of 0.1–0.2 vol%.

Finally, a concentration is only complete with its reference temperature. This industry works in vol% referenced to 60 °F (15.6 °C).

Fouling risk in PG, and prism condition diagnostics

Put honestly, PG plus refractometry is the most biologically active fluid paired with the most surface-sensitive method: critical-angle refractometry reads a layer about 1 µm thick at the prism face, so a film does not block the measurement, it grows inside it.

What answers that is the same detector. The position of the shadow line is the measurement; its sharpness and contrast are a second quantity seen at the same time. A film blunts the edge before it shifts the position, so the instrument can report its condition before the reading is visibly wrong, instead of quietly returning a plausible number.

StateWhat it meansAction
GoodEdge quality normal, concentration within specificationNone
DegradedEdge quality falling, concentration still within specificationSchedule a clean — this is the state worth having: maintenance gets planned before anyone sees a bad number
FailedConcentration can no longer be supportedThe instrument outputs refractive index and temperature and withholds concentration

Where the measuring point goes

  • Location: a bypass or sample loop on the CDU secondary side, taken from the pump outlet and returned to the pump inlet
  • Attitude: a vertical measuring chamber with the flow running upward
  • Prism: flush with the flow path, not recessed — the scouring action of the flow is part of keeping it clean
  • Orientation: the prism face must never point downward. This one is not negotiable
  • Filtration: where the fluid can carry abrasive particles, filter them out upstream. The detection window is a wear part
  • Small bore: a 1/2″–1″ bypass is 2″ or under, so use the PS7110-MT1 small-bore adapter
  • Split mounting: for panel mounting, use the PS7110-SY1 remote display so the electronics and the optical block do not share thermal mass
  • Many points: campus-scale loops can be managed centrally with the PS7110-SY2, up to 120 channels
  • Flow: a 2 L/min bypass is about 0.25 m/s. Flow here keeps the sample fresh and scours the prism; it plays no part in the measurement

Recommended solutions

Measurement pointPrincipleModels
Liquid-cooled main loop EG / PG concentrationTuning fork + PT1000PS7400
Immersion-cooling dielectric fluid densityTuning forkPS7400
Metro / commercial chiller secondary refrigerantTuning forkPS7400
Ice-storage brine concentrationTuning fork / ultrasonic SoSPS7400 / PS7020
CDU secondary-loop PG concentrationCritical-angle refractometryPS7110-B
Outdoor dry-cooler loop (can fall below 0 °C in winter)Critical-angle refractometryPS7110-C

Selection support for this industry

Industry FAQ

Do AI data centers need online ethylene glycol concentration monitoring?

It is necessary. AI data center liquid cooling (cold‑plate and immersion types) typically uses aqueous solutions of ethylene glycol (EG) or propylene glycol (PG), with concentrations ranging from 30% to 50%. The importance of precise concentration control: too low a concentration → insufficient freezing point, posing a risk of pipe freezing in northern winters; too high a concentration → increased viscosity, leading to higher pump energy consumption and reduced heat transfer efficiency.

Drift sources:

  1. Dilution due to system makeup water;
  2. Local concentration increases as the evaporative section under high load preferentially removes water;
  3. Slow oxidation and decomposition of ethylene glycol.

Recommendation: PS7400 tuning fork density meter (density accuracy ±0.001 g/cm³, convertible to concentration accuracy ±0.5%), installed in the main loop of the heat exchanger.

Tuning fork or refractometer for data-centre liquid cooling?

Start with the fluid, then look at accuracy.

An EG loop can take either. The PS7400 tuning fork measures density and converts to concentration through a built-in curve at ±0.5 vol%; it goes straight into the main line with no bypass, which is the least trouble. The PS7110 measures refractive index at ±0.1 vol% — an order of magnitude better — at the cost of a sample bypass and of keeping the prism clean. Where top-ups are frequent and the concentration has to stay inside a narrow band, that trade is worth making. Where the question is only whether the loop has drifted somewhere dangerous, the fork is enough.

A PG loop: refractometer or fork, but not sound velocity. See the next question.

One practical point that has nothing to do with the principle: an outdoor dry-cooler loop can fall below 0 °C in winter. The PS7110-B stops at 0 °C, so that duty needs the PS7110-C (−10 to 100 °C).

Can sound velocity measure concentration in a PG loop?

No. Sound velocity is monotonic in ethylene glycol over the working range, but in propylene glycol it folds back mid-range — the curve turns over, one sound velocity corresponds to two concentrations, and the instrument cannot tell which branch it is on. There is no acoustic route to PG, so the PS7020 sound-velocity method does not apply to a PG loop.

Refractive index is monotonic across the range for both EG and PG, so PG concentration goes to refractometry (PS7110) or to density (PS7400 tuning fork).

While we are here, a limitation of the optical route itself: refractive index cannot tell PG from EG. At 25 vol% the two differ by about 0.0002 RI, while 1 vol% of concentration is about 0.001 RI. So the make-up fluid has to be controlled — the instrument must be told which fluid it is reading rather than left to guess. Top a PG loop up with EG and the reading will look entirely reasonable.

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